北京钢研高纳科技股份有限公司,北京 100081
郝志博(1987—),男,博士,高级工程师;E-mail:386098874@qq.com
收稿:2026-09-12,
修回:2026-10-02,
录用:2026-10-10,
网络首发:2026-10-21,
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郝志博,李尚平,李知旂等.真空水平连铸高温合金底吹氩去除夹杂物机制[J].特殊钢,
Hao Zhibo,Li Shangping,Li Zhiqi,et al.Inclusion Removal Mechanism by Bottom-Blown Argon in Vacuum Horizontal Continuous Casting of Superalloys[J].Special Steel,
以FGH4097高温合金返回料为研究对象,基于2 t真空水平连铸装备,采用底吹氩工艺开展高纯熔炼实验,通过高温可视化原位观测记录了气泡上浮、穿越熔池界面及破裂全过程,结合热传导方程的有限差分数值模拟,系统研究了底吹氩条件下气泡对熔体温度场、黏度场的扰动规律及其对夹杂物携带去除的作用机制。实验发现,熔体温度是决定气泡界面穿越行为的关键因素:当温度处于1 550~1 500 ℃时,气泡因表面张力不足难以突破熔池顶部界面,上浮净化效率受限;当温度降至1 500 ℃以下时,气泡周围形成显著的热影响区,局部熔体黏度增大,增强了对夹杂物的黏附捕获能力,气泡能够以稳定形态携带夹杂物穿越界面并在真空环境下破裂,随后夹杂物被熔渣或坩埚壁吸附去除。数值模拟结果表明,气泡进入熔体后,其内部及周边区域在数秒内保持明显低于熔体的温度,形成径向温度梯度,对应黏度呈局部升高分布,与实验观测现象一致。研究揭示了气泡携带夹杂物上浮去除遵循热黏附、界面吸附与机械裹挟三重耦合机制,明确了温度场-黏度场-气泡行为协同作用下的夹杂物净化规律。该成果为真空水平连铸底吹氩工艺的温度区间选择、吹气参数优化及返回料高纯化处理提供了理论依据和工艺指导。
This study focuses on FGH4097 superalloy revert scrap. Based on a 2 t vacuum horizontal continuous casting facility, high-purity melting experiments were conducted with bottom-blowing argon. The entire process of argon bubble rising, crossing the melt pool interface, and bursting was recorded by high-temperature in-situ visual observation. By combining finite-difference numerical simulations of the heat conduction equation, the disturbance patterns of the temperature and viscosity fields caused by the bubbles and their influence on inclusion removal were systematically investigated. Experimental results show that melt temperature is the key factor governing bubble interfacial crossing behavior. In the range of 1 550 ℃–1 500 ℃, bubbles struggle to break through the top interface due to insufficient surface tension, leading to limited flotation purification efficiency. When the temperature drops below 1 500 ℃, a pronounced heat-affected zone forms around the bubbles, increasing the local melt viscosity, which enhances the adhesion and capture of fine inclusions. Bubbles can then stably carry inclusions across the interface and burst under vacuum, after which the inclusions are adsorbed by slag or crucible walls for removal. Numerical simulation results indicate that upon entering the melt, the bubble interior and its surrounding region maintain a significantly lower temperature than the bulk melt for several seconds, thereby forming a radial temperature gradient, with a corresponding localized increase in viscosity, which agrees well with experimental observations. The study reveals that inclusion removal by bubble flotation follows a triple coupling mechanism: thermal adhesion, interfacial adsorption, and mechanical entrapment. It clarifies the purification mechanism under the synergistic effect of temperature field, viscosity field, and bubble behavior. The findings provide a theoretical basis and process guidance for temperature range selection, argon blowing parameter optimization, and high-purity recycling of superalloy revert scrap in vacuum horizontal continuous casting.
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