西安钢研功能材料股份有限公司,西安 712046
王言眸(1995—),女,硕士,工程师; E-mail:1210776941@qq.com
收稿:2026-08-06,
修回:2026-09-05,
录用:2026-09-09,
网络首发:2026-09-30,
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王言眸,王祥,王旭等.单/双级时效对UNS R30003超薄钴基箔材组织与性能的调控[J].特殊钢,
Wang Yanmou,Wang Xiang,Wang Xu,et al.Regulation of Microstructure and Properties of UNS R30003 Ultra‑thin Cobalt‑based Foil by Single‑and Two‑stage Aging[J].Special Steel,
针对UNSR30003钴基弹性合金超薄箔材在经过大变形冷轧后残余应力高、塑性不足的问题,以97.4%累积变形量的0.1 mm超薄冷轧箔材为对象,研究了低温单级(450 ℃)、高温单级(500 ℃)及高低温双级(450 ℃+750 ℃)时效工艺对合金箔材微观组织、力学性能及V型弹簧弹性服役响应的调控规律。研究结果表明:冷轧态合金微观组织呈亚微米级层片状变形特征,畸变组织中贯穿多组变形晶粒的剪切带。450 ℃低温单级时效依靠细小弥散相与位错遗传使材料达到峰值强度(抗拉强度2 820 MPa,硬度549.23HV),但断后伸长率降至3.3%;500 ℃高温单级时效促使基体回复及析出相粗化,实现了强塑性的初步平衡。采用450 ℃×300 min+750 ℃×80 min双级时效工艺可有效兼顾强塑性;在保持1 600 MPa抗拉强度的同时,断后伸长率提升至6.7%(较冷轧态和低温单级时效分别提高19.64%和103.03%),且弹性模量(205 GPa)与抗弹性变形承载能力均优于冷轧态。双级时效通过分级析出与分段应力释放机制,诱导位错大幅重排并消除残余应力,实现了对合金箔材强度、塑性与弹性刚度的协同优化,为超薄精密弹性合金元件的热处理工艺制定提供依据。
Aiming at the problems of high residual stress and insufficient plasticity of UNSR30003 cobalt‑based elastic alloy ultra‑thin foils after large‑deformation cold rolling, the 0.1 mm ultra‑thin cold‑rolled foil with an accumulative deformation of 97.4% was taken as the research object. The regulation mechanisms of microstructures, mechanical properties and V‑spring elastic service response of alloy foils were investigated under three aging processes: low‑temperature single‑stage aging (450 ℃), high‑temperature single‑stage aging (500 ℃), and high‑low‑temperature two‑stage aging (450 ℃+750 ℃). The results show that the cold‑rolled alloy exhibits submicron lamellar deformed microstructures, and shear bands penetrating multiple deformed grains are observed within the distorted matrix. The low‑temperature single‑stage aging at 450 ℃ achieves the peak strength (ultimate tensile strength of 2 820 MPa, hardness of 549.23HV) via fine dispersed precipitates and inherited dislocations, whereas the elongation after fracture decreases to 3.3%. The high‑temperature single‑stage aging at 500 ℃ promotes matrix recovery and precipitate coarsening, yielding a preliminary strength‑ductility balance. The two‑stage aging process of 450 ℃×300 min+750 ℃×80 min can effectively balance strength and ductility; an ultimate tensile strength of 1 600 MPa is maintained while the elongation after fracture increases to 6.7%, which is 19.64% and 103.03% higher than those of the cold‑rolled state and the low‑temperature single‑stage aged state, respectively. Moreover, its elastic modulus (205 GPa) and resistance to elastic deformation are superior to those of the cold‑rolled foil. Through hierarchical precipitation and stepwise stress‑release mechanisms, two‑stage aging induces substantial dislocation rearrangement and relieves residual stress, realizing the synergistic optimization of strength, ductility and elastic stiffness of the alloy foil. This work provides a reference for formulating heat‑treatment procedures of ultra‑thin precision elastic alloy components.
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